Oral presentations from the 2010 FPRW meeting are linked below by blue and underlined text. Although the presentations were displayed via PowerPoint format during the meetings, they have been converted to Adobe PDF format to conserve space on this web server. Presentations are only posted with the speaker's written consent. Some speakers (for a variety of reasons - agency/company policy, copyrighted material, data in pre-pub status, etc) have elected not to post their presentation, and those files are not housed on this website. Some of the posted PDF files have security restrictions enabled (e.g. restriction of printing, copying text, etc), or selected slides deleted, per each speaker's request. If a link does not exist below, or if a linked file does not meet your needs, please contact the particular speaker directly (contact information is at the back of the 2010 Final Program).

 

 

2010 - 47th Florida Pesticide Residue Workshop

 

MEETING PROGRAM

 

Sunday Afternoon, July 18th

 

2:00 – 5:00 pm           Town Hall discussion forum on technical and managerial issues.

 

2:00 – 3:00 pm           Organic Analyses in Support of the Recent Gulf Coast Oil Spill -

                                        Leaders of Discussion: Dr. Ed Overton and Jack Cochran

 

3:00 – 3:30 pm           Anecdotes from Auditors and the Audited

 

3:30 – 4:00 pm           Anecdotes from Company Phone Service Representatives

 

4:00 – 5:00 pm           FDA’s Pesticide Monitoring Program: Overview, Regulatory and Analytical Challenges, and Guidance for Private Labs Conducting Pesticide Residue Analysis

 

5:00 – 9:00 pm           Technical Session Setup

5:00 – 10:00 pm         Exhibition Set-up

5:30 – 6:00 pm           Volunteers Orientation

6:00 – 6:30 pm           Moderator Training

6:00 – 8:00 pm           Registration

6:00 pm                        Poster Session Set up

7:00 – 8: 00 pm          Vendor Seminar: Restek Corporation

V-1                                 Enhancing That Certain Part of the GC Anatomy with QuEChERS and Cartridge SPE Cleanup for Pesticides in Dietary Supplements - Michelle Misselwitz

 

 

Monday Morning, July 19th

 

7:30 am - 5:00 pm     Registration

7:15 – 8:15 am           Vendor Breakfast Seminar: Waters Corporation

V-2                                 1) An Overview of Advanced MS Technologies for Residue Screening;

                                        2) UltraPerformance Residue Analysis using UPLC TQ MS;

                                        3) Capability of QTof for Target and Non-Targeted Screening in Food, Water and Wildlife Samples - Tim Jenkins

 

8:30 – 10:30 am         Opening Oral Session – Jack Cochran and Steve Lehotay, co-chairs

 

8:30 – 8:45 am           Welcome and opening announcements

 

8:45 – 9:20 am           Multiclass, Multiresidue Analysis of Pesticides Typically Analyzed in Single Analyte

O-1                                 Methods -

                                        Michelangelo Anastassiades; CVUA-Stuttgart, Fellbach, Germany

 

9:20 – 9:55 am           Multiclass, Multiresidue Analysis of Pesticides, Veterinary Drugs, Environmental

O-2                                 Contaminants, and Mycotoxins -

                                        Hans Mol; RIKILT, Wageningen, The Netherlands

 

9:55 – 10:30 am         How to Devise a “Greener” Lab and Facility –

O-3                                 Jonathan Friedan; Ballinger, Philadelphia, PA

 

10:30 am – noon       Exhibition Opening (with ribbon cutting ceremony)

 

11:00 am – noon       Poster Session for rest of day – Group A authors at posters

                                        Sarah McMullen and Paul Yang co-coordinators of poster sessions

 

Monday Afternoon,  July 19th

 

12:15 – 1:15 pm         Vendor Lunch Seminar: Thermo Fisher Scientific

V-3                                 EPA Method 1699: High Selective Multiresidue HRGC/HRMS Pesticide Analysis applied to food samples -Heinz Mehlmann

 

1:30 – 3:00 pm           Technical Session – Veterinary Drug Residue Analysis

                                        Sherri Turnipseed and Perry Martos (co-chairs)

Recent Studies on Veterinary Drug Residue Analysis Methods in My Lab

Steven Lehotay

 1:30 – 2:00 pm           Controlling Hormonal Residues in Animal Biological Matrices: from Conventional

O-4                                 Targeted Methods to Emerging Global “Omic” Approaches –

                                        Jean-Philippe Antignac; National Veterinary University of Nantes, France

 

2:00 – 2:30 pm           Analysis of Antiviral Drug Residues in Poultry and Swine by LC-MS/MS –

O-5                                 Mary Carson; FDA Center for Veterinary Medicine, Laurel, MD

 

2:30 – 3:00 pm           Improving Analytical Efficiencies in Single-Analyte Methods for Veterinary Drug

 O-6                                Residues in Foods of Animal Origin –

                                        Bryn Shurmer; Canadian Food Inspection Agency, Saskatoon, Canada

 

3:00 – 3:30 pm           Break for Exhibition and Posters

 

3:30 – 5:00 pm           Oral Session – What You Don’t Want to Know About QA and Lab Management but Can’t Avoid -

                                        Gail Parker, chair (Kevin Armbrust, co-chair)

 

3:30 – 4:00 pm           What You Always Wanted to Know About Root Cause Analysis and Managements

 O-7                                Review, but Were Afraid to Ask -

                                        Arlene Fox; AOAC International, Gaithersburg, MD

 

4:00 – 4:30 pm           ISO 17025, Section 5.9, or How I Learned to Stop Worrying and Love the Bomb -

O-8                                 Gail Parker; FL Dept. of Agriculture and Consumer Services, Tallahassee, FL; USA

 

4:30 – 5:00 pm           Statistics Without Math -

O-9                                 Barry Nussbaum; EPA Office of Environmental Information, Washington, DC

 

6:00 to 7:30 pm         Evening Reception sponsored by TradeWinds

 

Tuesday Morning,  July 20th

 

7:30 – 8:15 am           Early Morning Coffee in Exhibition Hall

 

7:15 – 8:15 am           Vendor Breakfast Seminar: Agilent Technologies

V-4                                 Analysis of Contaminants in Foodstuffs using the 7000 Series Tandem Quadrupole GC-MS System - Chris Sandy 

                                        Recent Developments in LC-MS/MS Analysis of Food Contaminants - Peter Stone

 

8:30 – 10:30 am         Oral Session – Global Chemical Contaminant Conflicts … and Resolutions

                                        Andrι de Kok and James Chang, co-chairs

 

8:30 – 9:00 am           Recent Developments in European Pesticide Registration and Impact on Global

O-10                              Trade -

                                        Monika Bross; BASF, Limburgerhof, Germany

 

9:00 – 9:30 am           Challenges for Governmental Pesticide Laboratories in Brazil/Latin America -

O-11                              Ionara Pizzutti; Federal University of Santa Maria, Brazil

 

9:30 – 10:00 am         Pre-Harvest Monitoring and Management of Pesticide Residues in India -

O-12                              Kaushik Banerjee; National Research Centre for Grapes, Pune, India

 

10:00 – 10:30 am       Monitoring of Pesticide Residues in Export Products of Plant Origin in China –

O-13                              Jianhua Wang – Shandong Exit & Entry Inspection and Quarantine Bureau, Qingdao, China

 

10:30 am – noon       Exhibition and Posters (all day); Danishes, coffee, and muffins will be served at 10:30 am

 

11:00 am – noon       Group B authors at posters

 

Tuesday Afternoon, July 20th

 

12:15 – 1:15 pm         Vendor Lunch Seminar: UCT, Inc.

V-5                                 The Chemical Principles of Solid Phase Extraction in Residue Analysis –

                                        Michael Telepchak

 

1:30 – 3:00 pm           Oral Session – Out of the Analytical Bubble, Why Are We Analyzing Chemical Residues Anyway?

                                        Kevin Armbrust, chair (Gail Parker co-chair)

 

1:30 – 2:00 pm           Pesticide Residue Analysis: Fifty Years of Accomplishments and Continuing Challenges

O-14                              James Seiber; University of California at Davis, CA

 

2:00 – 2:30 pm           Measuring Environmental Exposures: the Other Key to Risk Assessment -

O-15                              Keith Solomon; University of Guelph, Canada

 

2:30 – 3:00 pm           Helping the Farmer Helps the Regulator, Retailer, Consumer, and Environment: Everybody

O-16                              Wins -

                                        Danit Klein; Lab-Path, Ziona, Israel

 

3:00 – 3:30 pm           Break for Exhibition and Posters

3:30 – 5:00 pm           Forum on Mass Spectrometry: Hans Mol and Jean-Philippe Antignac will discuss in moderated debate format different approaches to make chemical residue identifications using MS techniques;

                                        Moderator: Sherri Turnipseed

 

5:30 – 7:00 pm           Organizing Committee Meeting

5:30 pm                        Beach Volleyball Game

 

Wednesday Morning,  July 21st

7:30 am – 4:30 pm    Registration

 

7:15 – 8:15 am           Vendor Breakfast Seminar: Pickering Labs

V-6                                 Keys to an Analytical Method: Focus on Mycotoxins

                                        Wendy Rasmussen and Bill Holmes (Mississippi State University)

 

7:30 – 8:15 am           Early Morning Coffee in Exhibition Hall

                                        International Travel Accommodation Talk:

 

8:30 – 8:50 am           Ambient Desorption Mass Spectrometry: A New Challenge in Rapid Pesticide Residues/

O-17                              Other Chemicals Control?

                                        Jana Hajslova, Institute of Chemical Technology; Prague, Czech Republic

 

8:50 am – noon         Oral Session - US Government in Action

                                        Lynda Podhorniak and Alaa Kamel, co-chairs

 

8:50 – 9:20 am           What’s New with the Pesticide Residue Program in the FDA?-

O-18                              Christopher Sack; FDA Total Diet Study Research Center, Lenexa, KS

 

9:20 - 9:40 am            Multiresidue Analysis of Pesticides in Botanical Dietary Supplements, Herbals and Dried

O-19                              Botanicals by GC-MS and LC-MS Techniques -

                                        Jon Wong; FDA Center for Food Safety and Applied Nutrition, College Park, MD

 

9:40 - 10:00 am          Determination of 200 Pesticides in 24 Food Matrices by Liquid Chromatography-Tandem

O-20                              Mass Spectrometry -

                                        Kai Zhang; FDA Center for Food Safety and Applied Nutrition, College Park, MD

 

10:00 – 10:30 am       Exhibition and Posters - Danishes, coffee, and muffins will be served at 10:00 am

                                        Final Votes by the Attendees for Best Poster are Due by Noon in the Ballot Box

 

10:30 – 11:00 am       Changes in the FSIS Field and Lab Operations on Residue Analysis –

O-21                              Terry Dutko - USDA Food Safety Inspection Service, St. Louis, MO

 

11:00 – 11:30 am       20-Year Retrospective and Update of the Pesticide Data Program -

O-22                              Diana Haynes; USDA Agricultural Marketing Service, Manassas, VA

 

11:30 am – noon       Risk Assessment and Monitoring Data - Historical Aspects -

O-23                              Susan Hummel; EPA Health Effects Division, Washington, DC

 

Wednesday Afternoon, July 21st

 

12:15 – 1:15 pm         Vendor lunch seminar: LECO Corporation

V-7                                 Comprehensive Two-Dimensional Gas Chromatography (GCxGC) Past and

                                        Present: Exploring its Effective Use as a Routine Analytical Technique -

                                        Joe Binkley and Mike Riley

 

 

1:30 – 4:30 pm           Oral Session - Cream of the Crop Technical Talks

                                        Alex Krynitsky and Steve Lehotay, co-chairs

 

1:30 – 1:50 pm           Targeted GC Pesticide Analysis at FDA: Transitioning to GC/MS/MS from GC/MS with

O-24                              Selected Ion Monitoring –

                                        Greg E. Mercer; FDA Pacific Regional Laboratory Northwest, Bothell, WA

 

1:50 – 2:10 pm           Practical Tools for GC-MS Analysis of Pesticides in Complex Matrices

O-25                              Katerina Mastovska; Covance Laboratories, Greenfield, IN

 

2:10 – 2:30 pm           Development of a Sample Preparation Method and Analytical Assay using LC-MS/MS

O-26                              for Quantitation of 10 Mycotoxins in a Single Analysis

                                        Lauryn E. Bailey – Eurofins Scientific, Metairie, LA

 

2:30 – 2:50 pm           Flow Injection Mass Spectrometry for High-Throughput Pesticide Residue Measurements

O-27                              Sergio C. Nanita - DuPont Crop Protection, Newark, DE

 

2:50 – 3:20 pm           Break

3:20 - 3:40 pm            Organochlorine Pesticides Determination in Strawberries and Jam using

O-28                              QuEChERS Extraction and GC-MS/MS –

                                        Valentina Domingues – Instituto Superior de Engenharia do Porto, Portugal

 

3:40 – 4:00 pm           Pesticide Residue Analysis of Catfish for the USDA-Pesticide Data Program (PDP)

O-29                              Jonathan Barber – USDA Agricultural Marketing Service, Gastonia, NC

 

4:00 – 4:20 pm           Determination of Three Neonicotinoids and their Metabolites in Pollen and Nectar of

O-30                              Field Treated Pumpkin to Assess their Potential Exposure to Honey Bees

                                        Alaa Kamel – EPA Office of Pesticide Programs, Fort George G. Meade, MD

 

4:20 – 4:30 pm           Poster award at close of meeting, thanks, and farewells

                                        Meeting Adjourns

 

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Last modified: August 30, 2010